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Haven't you heard of rigor mortis? Freezing the limb will also help, though of course when the limb thaws it will then melt due to cell membrane rupture from the expanding frozen water.
Clearly, however, the ideal solution is to tie a pair of deflated lungs together and use them to garrote your foes. The irony is a killer even if the weapon isn't.
My, this has become rather macabre rather quickly!
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